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Chem 233 UPDATED Test Questions and CORRECT Answers
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Purpose of Lab 10 Phenacetin is prepared by Williamson Ether Synthesis using acetaminophen (an ingredient in Tylenol), and iodoethane in the presence of a base. The product is purified by recrystallization and characterized by TLC, melting point analysis, and IR and NMR spectroscopies. (10) 2-butanone safety considerations Is highly flammable. Dispose of in appropriately labeled waste bottles. (10) Ethyl acetate safety considerations Is highly flammable. Dispose of in appropriately labeled waste bottles. (10) Iodoethane safety considerations It is toxic and corrosive. Measure and add to reaction in the fume hood. Wear gloves at all times when handling and wash affected areas thoroughly with water.
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