SOLUTION MANUAL
Analysis, Synthesis, and Design of Chemical Processes, 5th Edition
By Richard Turton, Joseph Shaeiwitz
LU
XE
LI
BR
AR
Y
, Table of Content
1. Diagrams for Understanding Chemical Processes
2. The Structure and Synthesis of Process Flow Diagrams
3. Batch Processing
4. Chemical Product Design
5. Tracing Chemicals through the Process Flow Diagram
6. Understanding Process Conditions
Section II: Engineering Economic Analysis of Chemical Processes
8. Estimation of Manufacturing Costs
9. Engineering Economic Analysis
10. Profitability Analysis
LU
Section III: Synthesis and Optimization of Chemical Processes
11. Utilizing Experience-Based Principles to Confirm the Suitability of a Process Design
12. Synthesis of the PFD from the Generic BFD
13. Synthesis of a Process Using a Simulator and Simulator Troubleshooting
XE
14. Process Optimization
15. Pinch Technology
16. Advanced Topics Using Steady-State Simulators
17. Using Dynamic Simulators in Process Design
18. Regulation and Control of Chemical Processes with Applications Using Commercial
LI
Software
Section IV: Process Equipment Design and Performance
19. Fluid Mechanics
BR
20. Heat Transfer
21. Separations
22. Reactors
23. Other Equipment
AR
24. Process Troubleshooting and Debottlenecking
Section V: The Impact of Chemical Engineering Design on Society
25. Ethics and Professionalism
26. Health, Safety, and the Environment
27. Green Engineering
Y
Section VI. Interpersonal and Communication Skills
28. Teamwork
, Chapter 1
1.1 Block Flow Diagram (BFD)
Process Flow Diagram (PFD)
Piping and Instrument Diagrams (P&ID)
(a) PFD
LU
(b) BFD
(c) PFD or P&ID
(d) P&ID
(e) P&ID
XE
1.2 P&ID
1.3 It is important for a process engineer to be able to review a 3-dimensional model prior to
the construction phase to check for clearance, accessibility, and layout of equipment,
piping, and instrumentation.
LI
1.4 (1) Clearance for tube bundle removal on a heat exchanger.
BR
(2) NPSH on a pump – affects the vertical separation of feed vessel and pump inlet.
(3) Accessibility of an instrument for an operator – must be able to read a PI or
change/move a valve.
(4) Separation between equipment for safety reasons – reactors and compressors.
(5) Crane access for removing equipment.
(6) Vertical positioning of equipment to allow for gravity flow of liquid.
AR
(7) Hydrostatic head for thermosiphon reboiler – affects height of column skirt.
1.5 Plastic models are no longer made because they are too expensive and difficult to
change/revise. These models have been replaced with virtual/E-model using 3-D CAD.
Both types of model allow revision of critical equipment and instrument placement to
Y
ensure access, operability, and safety.
1.6 Another reason to elevate the bottom of a tower is to provide enough hydrostatic head
driving force to operate a thermosiphon reboiler.
1-1
, 1.7 (a) PFD or P&ID
(b) PFD
(c) PFD
(d) P&ID
(e) BFD (or all PFDs)
1.8 A pipe rack provides a clear path for piping within and between processes. It keeps piping
off the ground to eliminate tripping hazards and elevates it above roads to allow vehicle
LU
access.
1.9 A structure – mounted vertical plant layout is preferred when land is at a premium and the
process must have a small foot print. The disadvantage is that it is more costly because of
the additional structural steel.
XE
1.10 (a) BFD – No change
PFD – Efficiency changed on fired heater, resize any heat exchanger used to extract
heat from the flue gas (economizer)
P&ID – Resize fuel and combustion air lines and instrumentation for utilities to fired
LI
heater. Changes for design changed of economizer (if present)
(b) BFD – Change flow of waste stream in overall material balance
PFD – Change stream table
BR
P&ID – Change pipe size and any instrumentation for this process line
(c) BFD – No change
PFD – Add a spare drive, e.g. D-301 → D-301 A/B
P&ID – Add parallel drive
(d) BFD – No change
PFD – No change
AR
P&ID – Note changes of valves on diagram
1.11 (a) A new vessel number need not be used, but it would be good practice to add a letter to
donate a new vessel, e.g. V-203 → V-203N. This will enable an engineer to locate the
new process vessel sheet and vendor information.
Y
(b) P&ID definitely
PFD change/add the identifying letter.
1-2
Analysis, Synthesis, and Design of Chemical Processes, 5th Edition
By Richard Turton, Joseph Shaeiwitz
LU
XE
LI
BR
AR
Y
, Table of Content
1. Diagrams for Understanding Chemical Processes
2. The Structure and Synthesis of Process Flow Diagrams
3. Batch Processing
4. Chemical Product Design
5. Tracing Chemicals through the Process Flow Diagram
6. Understanding Process Conditions
Section II: Engineering Economic Analysis of Chemical Processes
8. Estimation of Manufacturing Costs
9. Engineering Economic Analysis
10. Profitability Analysis
LU
Section III: Synthesis and Optimization of Chemical Processes
11. Utilizing Experience-Based Principles to Confirm the Suitability of a Process Design
12. Synthesis of the PFD from the Generic BFD
13. Synthesis of a Process Using a Simulator and Simulator Troubleshooting
XE
14. Process Optimization
15. Pinch Technology
16. Advanced Topics Using Steady-State Simulators
17. Using Dynamic Simulators in Process Design
18. Regulation and Control of Chemical Processes with Applications Using Commercial
LI
Software
Section IV: Process Equipment Design and Performance
19. Fluid Mechanics
BR
20. Heat Transfer
21. Separations
22. Reactors
23. Other Equipment
AR
24. Process Troubleshooting and Debottlenecking
Section V: The Impact of Chemical Engineering Design on Society
25. Ethics and Professionalism
26. Health, Safety, and the Environment
27. Green Engineering
Y
Section VI. Interpersonal and Communication Skills
28. Teamwork
, Chapter 1
1.1 Block Flow Diagram (BFD)
Process Flow Diagram (PFD)
Piping and Instrument Diagrams (P&ID)
(a) PFD
LU
(b) BFD
(c) PFD or P&ID
(d) P&ID
(e) P&ID
XE
1.2 P&ID
1.3 It is important for a process engineer to be able to review a 3-dimensional model prior to
the construction phase to check for clearance, accessibility, and layout of equipment,
piping, and instrumentation.
LI
1.4 (1) Clearance for tube bundle removal on a heat exchanger.
BR
(2) NPSH on a pump – affects the vertical separation of feed vessel and pump inlet.
(3) Accessibility of an instrument for an operator – must be able to read a PI or
change/move a valve.
(4) Separation between equipment for safety reasons – reactors and compressors.
(5) Crane access for removing equipment.
(6) Vertical positioning of equipment to allow for gravity flow of liquid.
AR
(7) Hydrostatic head for thermosiphon reboiler – affects height of column skirt.
1.5 Plastic models are no longer made because they are too expensive and difficult to
change/revise. These models have been replaced with virtual/E-model using 3-D CAD.
Both types of model allow revision of critical equipment and instrument placement to
Y
ensure access, operability, and safety.
1.6 Another reason to elevate the bottom of a tower is to provide enough hydrostatic head
driving force to operate a thermosiphon reboiler.
1-1
, 1.7 (a) PFD or P&ID
(b) PFD
(c) PFD
(d) P&ID
(e) BFD (or all PFDs)
1.8 A pipe rack provides a clear path for piping within and between processes. It keeps piping
off the ground to eliminate tripping hazards and elevates it above roads to allow vehicle
LU
access.
1.9 A structure – mounted vertical plant layout is preferred when land is at a premium and the
process must have a small foot print. The disadvantage is that it is more costly because of
the additional structural steel.
XE
1.10 (a) BFD – No change
PFD – Efficiency changed on fired heater, resize any heat exchanger used to extract
heat from the flue gas (economizer)
P&ID – Resize fuel and combustion air lines and instrumentation for utilities to fired
LI
heater. Changes for design changed of economizer (if present)
(b) BFD – Change flow of waste stream in overall material balance
PFD – Change stream table
BR
P&ID – Change pipe size and any instrumentation for this process line
(c) BFD – No change
PFD – Add a spare drive, e.g. D-301 → D-301 A/B
P&ID – Add parallel drive
(d) BFD – No change
PFD – No change
AR
P&ID – Note changes of valves on diagram
1.11 (a) A new vessel number need not be used, but it would be good practice to add a letter to
donate a new vessel, e.g. V-203 → V-203N. This will enable an engineer to locate the
new process vessel sheet and vendor information.
Y
(b) P&ID definitely
PFD change/add the identifying letter.
1-2