Aim: to test the boiling point of ethyl ethanoate.
Practical Part
We used the following equipment to perform this practical:
• Ethyl ethanoate
• Test tube
• Thermometer
• Rubber band
• Water bath
• Bunsen burner
Results
Temperatures were noted when:
Boiling point of the given
The evolution of gas bubbles
Rapid continuous evolution organic liquid (t1 + t2) / 2 (°C)
just stops t2 (°C) (after
of gas bubbles occurs t1 (°C)
removing from the flame)
78°C 84°C 81°C
Calculation and Results of Ethyl Ethanoate % Yield
Density gcm-1 Volume Used cm3 Mass Used g
Ethanol 0.789g/cm3 9cm3 7.101g
Ethanoic Acid 1.05g/cm3 5cm3 5.25g
Number of Moles Limiting Substance
Ethanol 7.101/46= 0.154
Ethanoic Acid 5.25/60= 0.0875 Yes, due to least amount of moles
Theoretical 100% Yield Calculation:
The reaction can produce 0.0875 moles of ethyl
Mass Ethanoic Acid = 5.25g
ethanoate by a 100% reaction
Mr Ethanoic Acid = 60 What would this mass be?
Number of Moles Ethanoic Acid = 0.0875 Mass = (Moles * Mr) 0.0875 * 77 = 6.7375
5.0cm3 Ethanoic Acid = 0.0875 moles Theoretical 100% yield mass = 6.74