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Exam (elaborations)

Solutions Manual for Analysis, Synthesis, and Design of Chemical Processes, 3rd Edition

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This comprehensive solutions manual accompanies the third edition of Analysis, Synthesis, and Design of Chemical Processes. It provides detailed, step-by-step solutions to problems covering key topics in chemical engineering, including process flow diagrams (PFDs), piping and instrumentation diagrams (P&IDs), batch and continuous processes, reactor design, distillation, process economics, and profitability analysis. With chapters dedicated to equipment sizing, cost estimation, energy integration, and economic evaluation, this manual is an essential resource for students, instructors, and practicing engineers seeking to deepen their understanding of chemical process design and optimization.

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Analysis, Synthesis, and Desi
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Uploaded on
November 26, 2025
Number of pages
578
Written in
2025/2026
Type
Exam (elaborations)
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,
, Chapter 1 x




1.1 Block Flow Diagram (BFD)
x x x



Process Flow Diagram (PFD)
x x x x



Piping and Instrument Diagrams (P&ID)
x x x x




(a) PFD
(b) BFD
(c) PFD or P&ID x x



(d) P&ID
(e) P&ID


1.2 P&ID


1.3 It is important for a process engineer to be able to review a 3-dimensional model prior to
x x x x x x x x x x x x x x x x



the construction phase to check for clearance, accessibility, and layout of equipment,
x x x x x x x x x x x x



piping, and instrumentation.
x x x




1.4 (1) Clearance for tube bundle removal on a heat exchanger.
x x x x x x x x x



(2) NPSH on a pump – affects the vertical separation of feed vessel and pump inlet.
x x x x x x x x x x x x x x



(3) Accessibility of an instrument for an operator – must be able to read a PI or x x x x x x x x x x x x x x x



change/move a valve.
x x x



(4) Separation between equipment for safety reasons – reactors and compressors.
x x x x x x x x x



(5) Crane access for removing equipment. x x x x



(6) Vertical positioning of equipment to allow for gravity flow of liquid.
x x x x x x x x x x



(7) Hydrostatic head for thermosiphon reboiler – affects height of column skirt. x x x x x x x x x x




1.5 Plastic models are no longer made because they are too expensive and difficult to
x x x x x x x x x x x x x



change/revise. These models have been replaced with virtual/E-model using 3-D CAD.
x x x x x x x x x x x



Both types of model allow revision of critical equipment and instrument placement to
x x x x x x x x x x x x x



ensure access, operability, and safety.
x x x x x




1.6 Another reason to elevate the bottom of a tower is to provide enough hydrostatic head
x x x x x x x x x x x x x x



driving force to operate a thermosiphon reboiler.
x x x x x x x




1-1

, 1.7 (a) x PFD or P&ID
x x x



(b) PFD
(c) PFD
(d) P&ID
(e) BFD (or all PFDs) x x x




1.8 A pipe rack provides a clear path for piping within and between processes. It keeps piping
x x x x x x x x x x x x x x x



off the ground to eliminate tripping hazards and elevates it above roads to allow vehicle
x x x x x x x x x x x x x x x



access.
x




1.9 x A structure – mounted vertical plant layout is preferred when land is at a premium and the
x x x x x x x x x x x x x x x x



x process must have a small foot print. The disadvantage is that it is more costly because of
x x x x x x x x x x x x x x x x



x the additional structural steel.
x x x




1.10 (a) x BFD – No change
x x x x



PFD – Efficiency changed on fired heater, resize any heat exchanger used to extract
x x x x x x x x x x x x



heat from the flue gas (economizer) x x x x x x



P&ID – Resize fuel and combustion air lines and instrumentation for utilities to fired
x x x x x x x x x x x x x



heater. Changes for design changed of economizer (if present) x x x x x x x x x



(b) BFD – Change flow of waste stream in overall material balance x x x x x x x x x



PFD – Change stream table
x x x x x



P&ID – Change pipe size and any instrumentation for this process line
x x x x x x x x x x x



(c) BFD – No change x x



PFD – Add a spare drive, e.g. D-301  D-301 A/B x x x x x x x x x



P&ID – Add parallel drive
x x x x x



(d) BFD – No change x x



PFD – No change
x x x



P&ID – Note changes of valves on diagram x x x x x x x




1.11 x (a) A new vessel number need not be used, but it would be good practice to add a letter
x x x x x x x x x x x x x x x x x x



to donate a new vessel, e.g. V-203  V-203N. This will enable an engineer to locate
x x x x x x x x x x x x x x x x



the new process vessel sheet and vendor information.
x x x x x x x x



(b) P&ID definitely
x x



PFD change/add the identifying letter. x x x x




1-2

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