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Exam (elaborations)

Instrumental Analysis – Exam 1 Questions with Verified Answers – Core Concepts and Principles Explained

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This document presents a curated set of verified questions and concise answers for Exam 1 in Instrumental Analysis, covering foundational concepts such as Beer's Law, laser operation, types of electrical and data domains, detector mechanisms, and common noise types. It includes theoretical definitions and practical instrument setup components. Ideal for early-course review and reinforcement of analytical instrumentation basics.

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Institution
Instrumental Analysis
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Instrumental Analysis

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Uploaded on
June 6, 2025
Number of pages
8
Written in
2024/2025
Type
Exam (elaborations)
Contains
Questions & answers

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Instrumental Analysis - Exam 1 questions with
verified answers
+/- of bunching Ans✓✓✓ +: draws line of best fit to get better
determination of signal


-: can use to much and toss peaks which were signal and not noise


3 electrical domains Ans✓✓✓ 1. analog (encoded as a magnitude of
electrical quantities)
2. time - signal fluctuations per unit time (a frequency reading)
3. digital (most common, usually a computer)


Beer's Law Ans✓✓✓


Black body radiation Ans✓✓✓ aka thermal radiation


creates continuous spectrum, radiation from temp of surface,
oscillations in excited solids)


bunching Ans✓✓✓ averaging certain # points into one point on
spectrum

, chemical noise vs instrumental noise Ans✓✓✓ chemical =
uncontrollable (temp, pressure, etc.)


instrumental = from components of instrument (thermal, shot, flicker,
environmental)


Components of optical instruments Ans✓✓✓ 1. stable source of
radiant energy
2. transparent container for holding sample
3. device for isolating desired region of spectrum
4. radiator detector
5. signal processor and readout


continuum energy sources Ans✓✓✓ emit radiation that changes
intensity slowly as a function of wavelength


data domains Ans✓✓✓ modes of encoding, going from one system to
another to extract information


detection limit Ans✓✓✓ minimum Amt of analyte that can be detected
with known confidence i.e. how little do i need to detect anything

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