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Analytical Chemistry – Exam Graded A+

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This document contains exam material for Analytical Chemistry, focused on key concepts and topics relevant to course assessment. It is designed to support students in reviewing analytical chemistry principles and preparing for examinations, with content associated with an A+ graded exam.

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ANALYTICAL CHEMISTRY




ANALYTICAL CHEMISTRY EXAM GRADED A+



ANALYTICAL CHEMISTRY - correct answer Branch of chemistry that deals
with the separation, identification and composition of matter


Gravimetric Method - correct answer Measurement of mass of substance
that is chemically related to the analyte


Volumetric Method - correct answer Measures the volume of solution
necessary to read completely with the analyte.


Spectroscopic Method - correct answer Measures the electromagnetic
radiation produced by the analyte or its interactions with it.

, ANALYTICAL CHEMISTRY


Electroanalytic Method - correct answer Measures the electrical properties
of the analyte such as current, potential, resistance, and amount of
charge


Kjeldahl Method - correct answer Determination of Organic Nitrogen
(Amines, Amides, Nitriles and Nitro Group: %N or %Protein


Double Indicator Method - correct answer To determine the composition of
a soda ash sample. Two indicators (one alkaline range one acidic)
Example: Phenolphthalein endpoint (Na2CO3 and NaOH) and methyl
red endpoint (Na2CO3 and NaHCO3)


Argentometric titration - correct answer Titration with Silver Nitrate AgNO3


Mohr Method - correct answer Direct method for halides and cyanides;
Titration is carried out between pH of 7-10. Usually, a low concentration
of chromate is desired to detect the end point clearly since a chromate
ion imparts an intense yellow color.


Volhard Method - correct answer For the formation of a colored
complexion; Direct method for silver; Indirect method for halides;
Titration is carried out in acidic condition to hasten precipitation of
ferric ion to its hydrated oxide form.


Fajan's Method - correct answer For the formation of a colored adsorption
complex; same as Mohr's but uses DCF dichlorofluorescein; between pH

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