Volume 35
,.......
Board of Directors
THOMAS B. RAUCHFUSS, president University of Illinois at Urbana-Champaign
DIMITRI COUCOUVANIS University of Michigan
MARCETTA Y. DARENSBOURG Texas A&M University
JOHN R. SHAPLEY University of Illinois at Urbana-Champaign
Secretary to the Corporation
STANTON CHING Connecticut College
Future Volumes
36 GREGORY S. GIROLAMI and ALFRED P. SATTELBERGER University of Illinois
at Urbana-Champaign and Argonne National Laboratory
37 PHILIP P. POWER University of California at Davis
International Associates
MARTIN A. BENNETT Australian National University
FAUSTO CALDERAZZO University of Pisa
M. L. H. GREEN Oxford University
JACK LEWIS Cambridge University
RENE POILBLANC University of Toulouse
HERBERT W. ROESKY University of Göttingen
WARREN R. ROPER University of Auckland
F. G. A. STONE Baylor University
JAN REEDIJK Leiden University
H. VAHRENKAMP University of Freiburg
AKIO YAMAMOTO Tokyo Institute of Technology
,Editor-in-Chief
THOMAS B. RAUCHFUSS
University of Illinois at Urbana-Champaign
.................................................................
INORGANIC
SYNTHESES
Volume 35
, Copyright Ó 2010 by John Wiley & Sons, Inc. All rights reserved
Published by John Wiley & Sons, Inc., Hoboken, New Jersey
Published simultaneously in Canada
No part of this publication may be reproduced, stored in a retrieval system, or transmitted in any
form or by any means, electronic, mechanical, photocopying, recording, scanning, or otherwise,
except as permitted under Section 107 or 108 of the 1976 United States Copyright Act, without
either the prior written permission of the Publisher, or authorization through payment of the
appropriate per-copy fee to the Copyright Clearance Center, Inc., 222 Rosewood Drive, Danvers,
MA 01923, (978) 750-8400, fax (978) 750-4470, or on the web at www.copyright.com. Requests to
the Publisher for permission should be addressed to the Permissions Department, John Wiley &
Sons, Inc., 111 River Street, Hoboken, NJ 07030, (201) 748-6011, fax (201) 748-6008, or online at
http://www.wiley.com/go/permission.
Limit of Liability/Disclaimer of Warranty: While the publisher and author have used their best
efforts in preparing this book, they make no representations or warranties with respect to the
accuracy or completeness of the contents of this book and specifically disclaim any implied
warranties of merchantability or fitness for a particular purpose. No warranty may be created or
extended by sales representatives or written sales materials. The advice and strategies contained
herein may not be suitable for your situation. You should consult with a professional where
appropriate. Neither the publisher nor author shall be liable for any loss of profit or any other
commercial damages, including but not limited to special, incidental, consequential, or other
damages.
For general information on our other products and services or for technical support, please contact
our Customer Care Department within the United States at (800) 762-2974, outside the United
States at (317) 572-3993 or fax (317) 572-4002.
Wiley also publishes its books in a variety of electronic formats. Some content that appears in print
may not be available in electronic formats. For more information about Wiley products, visit our
web site at www.wiley.com.
Library of Congress Catalog Number: 39:23015
ISBN 978-0471-68255-4
Printed in the United States of America
10 9 8 7 6 5 4 3 2 1